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'Super-microscope' opens at Isis

By James Morgan

Science reporter, BBC News

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Inside the giant microscope - Martyn Bull from Isis shows us around

The world's newest "super microscope" is fired up and ready to go.

The 200m second target station at Isis in Oxfordshire will allow scientists to

see things 10,000 times thinner than a human hair.

The machine is known as a pulsed neutron source. But what does that actually

mean?

Well, if you're a physicist curious to see how matter behaves when no-one is

looking, then Isis is your private snoop.

If you're an engineer trying to make the hydrogen car a working reality, then

Isis is your genie.

World leader

Want to see how spiders spin silk stronger than steel? Or peer into a newborn

baby's lungs as they take their first breath?

Isis will grant your wishes - and you get more than three. Up to 40 different

experiments can run side by side, now that the second target station "Isis 2"

is open.

No wonder that physicists from across the globe will be flying in to seek an

audience with the oracle, which resides at the Rutherford Appleton Laboratory,

at Harwell Science and Innovation Campus.

Their areas of interest stretch the breadth of the Universe - from the darkest

corners of quantum mechanics, to the supermarket shelf.

Theory geeks searching for the elusive "Boson peak" will stand side-by-side

with a Dutch group who are studying cheese.

Both groups have turned to neutron scattering as a powerful tool for examining

their materials at the atomic level - the positioning, spacing, and the forces

between the individual atoms.

"Essentially, it's a giant camera," says Andrew Taylor, the Director of Isis,

which is owned and operated by the Science and Technology Facilities Council

(STFC).

"Let's do a simple experiment - take your Biro pen and bend it. What do you

see? One side stretches and the other contracts - the individual atoms are

getting closer or further apart.

"Now imagine your pen is the turbine blade of a Rolls Royce jet engine -

operating under vast mechanical and thermal stresses.

"Isis allows you to measure these stresses, and see how they alter the spacing

between each individual atom of the turbine.

"And you're not just taking a snapshot - you can watch how this changes over

time, with temperature, or any other variable.

"You're not just sending a postcard; you're making a little video story."

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Timelapse: Building the new target station

The first target station, Isis 1, has exceeded all expectations since it opened

in 1984.

It has answered fundamental questions - about magnetism at the atomic level, or

the properties of "Buckyballs" - synthetic carbon molecules, once hailed as the

great hope of nanotechnology.

But equally, it has solved "everyday" problems - the causes of railway crashes,

or the most economic way to make fabric softener.

New frontiers

The second target station will open new frontiers - soft condensed matter,

bio-molecular sciences, and advanced materials.

SPYING ON ATOMS

"Throughout the 90s, it became apparent that there was some science that we

just couldn't do with Isis 1," said Andrew Taylor.

"We wanted to look at polymers, surfactants, aggregates - these things have got

structures bigger than just a few tenths of angstroms.

"Bigger molecules need neutrons which are matched to their structure - longer

wavelength neutrons."

The new target station supplies these. It also has a greater flux (flow of

neutrons per second) allowing greater control of intensity, and quicker

experiments - ideal if you are a researcher visiting from Japan for just three

days of beam time.

At its core is a lump of tungsten metal the size of a packet of biscuits - the

"target" - into which pulses of protons are fired at 84% of the speed of light.

The target radiates neutrons like a discoball scatters light - 20,000 million

million per second.

Surrounding it is a ring of colour-coded bunkers, inside which scientists place

their samples - be they toothpaste or turbine blades.

Each bunker houses a different experimental tool for imaging matter.

The neutrons are like pinballs fired into the sample, cannoning off the atoms

inside and spraying out on to a detector.

By recording the angles they pop out, scientists can plot the atomic structure

of the sample material, without breaking it open, or cutting it up.

And whereas other high-resolution microscopy techniques only scratch the

surface of a material, Isis can give a cross sectional view of the material in

its natural state.

Take a pint of beer. To watch the individual alcohol molecules flirting with

different water molecules, you need to observe them in the aqueous environment.

Spiders and silkworms spin their silk from liquid precursors - creating fibres

far stronger than anything we humans can synthesise artificially. So how do

they do it?

Scientists from the Oxford Silk Group have been using Isis 1 to measure the

properties of the liquid silk ingredients.

Isis 2 is equipped with more powerful experiments, which will reveal how the

silk recipe is stored and prepared.

Meanwhile, on a global scale, the new target station will help Isis to compete

with other neutron sources.

They include the Institut Laue-Langevin (ILL), Grenoble, France, which uses a

continuous nuclear reactor as its neutron source, and the Spallation Neutron

Source (SNS), in Oak Ridge, Tennessee, US, which is based on Isis technology,

only with higher beam powers.

Rival machines

But is neutron scattering really so special? After all, there are other types

of super-microscope - one within eyesight of Isis.

The Diamond synchrotron light source uses highly focused beams of X-rays to

probe deep into the basic structure of matter and materials.

But Isis can do some things that Diamond just cannot.

"We see matter in a different way," Andrew Taylor explains. "Neutrons see the

nucleus of the atom. X-rays see the electrons.

"And that means that neutrons see the hydrogens. X-rays don't.

"Take uranium hydride. Uranium's got 92 electrons and hydrogen has one. The

X-rays have no idea where the hydrogen is.

"But neutrons see the hydrogen and uranium nuclei with equal magnitude."

No wonder that automotive engineers aiming to design hydrogen storage materials

are working with Isis.